nav emailalert searchbtn searchbox tablepage yinyongbenwen piczone journalimg journalInfo journalinfonormal searchdiv searchzone qikanlogo popupnotification paper paperNew
2025, 06, v.22 664-674
二维核磁共振测井在页岩储层评价中的应用
基金项目(Foundation): 中石化石油工程公司项目(编号:SG23-54K)
邮箱(Email):
DOI:
摘要:

采用P型核磁在黔北地区AX页岩气工区开展了两种模式二维核磁共振测井,根据横向弛豫谱峰(T2)分布特征和天然气信号特征进行了测量模式优选。对比了研究区与邻区储层地质特征,参考邻区核磁共振测井实验数据,结合实测谱峰特征,合理选取T2截止值进行核磁数据处理,开展了龙马溪组一段富有机质页岩储层孔隙度参数计算、孔隙结构分析,流体组分识别等工作,其中龙一1~1-龙一1~2底部层段核磁有效孔隙度平均4.8%,储层大孔径主要分布在在32~256 ms之间,T2-T1交会可动气区域信号最强,评为Ⅰ类储层。结合常规测井分析结果,证实了(T2-T1)二维核磁共振测井技术在低孔隙度页岩气储层测井评价中的准确性和适用性。结合元素测井计算的黄铁矿含量,简要分析了黄铁矿对核磁共振测井信号可能的影响作用,研究成果对类似地质条件下的页岩储层二维核磁共振测井评价提供了一定的参考作用。

Abstract:

Two modes of 2D nuclear magnetic resonance logging were conducted using P-type nuclear magnetic resonance in the AX shale gas work area in northern Guizhou. The measurement mode was optimized based on the distribution characteristics of transverse relaxation spectrum peaks and natural gas signal features. By comparing the geological characteristics of the reservoir in the study area with those in the neighboring area, referring to the experimental data of nuclear magnetic resonance logging in the neighboring area, and combining with the measured spectral peak characteristics, the T2 cut-off value was reasonably selected for nuclear magnetic data processing. The porosity parameters calculation, pore structure analysis, and fluid component identification of the organic rich shale reservoir in the first member of Longmaxi Formation were carried out. The average nuclear magnetic effective porosity was 4.8% of the layer S_1l1 and bottom of S_1l2, and the large pore size of the reservoir was mainly distributed between 32~256 ms. The signal in the T2-T1 intersection movable gas area was the strongest, and it was rated as a class I reservoir. Combined with conventional logging analysis results, the accuracy and applicability of the(T2-T1) 2D nuclear magnetic resonance logging technology in the logging evaluation of low porosity shale gas reservoirs have been confirmed. Based on the calculation of pyrite content using elemental logging, a brief analysis was conducted on the possible impact of pyrite on nuclear magnetic resonance logging signals. The research results provide a certain reference for the 2D nuclear magnetic resonance logging evaluation of shale reservoirs under similar geological conditions.

参考文献

[1] Coates G R,Xiao L Z,Prammer M G.NMR logging principles and applications[M].Texas:Gulf Publishing Company,1999.

[2] 胡法龙,周灿灿,李潮流,等.基于弛豫-扩散的二维核磁共振流体识别方法[J].石油勘探与开发,2012,39(5):552-558.Hu F L,Zhou C C,Li C L,et al.Fluid identification method based on 2D diffusion-relaxation nuclear magnetic resonance(NMR)[J].Petroleum Exploration and Development,2012,39(5):552-558.

[3] 佘刚,徐永发,李世毅,等.二维核磁共振测井在柴达木盆地复杂储层流体识别中的应用[J].地球物理学进展,2018,33(4):1 566-1 572.She G,Xu Y F,Li S Y,et al.Application of 2D NMR logging on complex reservoir fluid identification in Qaidam Basin[J].Progress in Geophysics,2018,33(4):1 566-1 572.

[4] 谭茂金,赵文杰,范宜仁.用测井双TW观测数据识别储层流体性质[J].天然气工业,2006,26(4):38-40.Tan M J,Zhao W J,Fan Y R.Identification of fluid property with nmr dual-TW well logging data[J].Natural Gas Industry,2006,26(4):38-40.

[5] 刘忠华,李霞,赵文智,等.核磁共振增强扩散方法在复杂储集层流体识别中的应用[J].石油勘探与开发,2010,37(6):703-708.Liu Z H,Li X,Zhao W Z,et al.Enhanced diffusion theory of nuclear magnetic resonance (NMR) and its application to fluid identification of complex reservoirs[J].Petroleum Exploration and Development,2010,37(6):703-708.

[6] 谢然红,肖立志.(T2,D)二维核磁共振测井识别储层流体的方法[J].地球物理学报,2009,52(9):2 410-2 418.Xie R H,Xiao L Z.The (T2,D) NMR losgins method for fluids characterization[J].Chinese Journal of Geophysics,2009,52(9):2 410-2 418.

[7] Sun B,Dunn K J.Core analysis with two dimensional NMR [C]//2002 International Symposium of the Society of Core Analysts.Monterey,USA:SCA,2002:22-25.

[8] Hürlimann M D,Venkataramanan L.Quantitative measurement of two-dimensional distribution functions of diffusion and relaxation in grossly inhomogeneous fields[J].Journal of Magnetic Resonance,2002,157(1):31-42.

[9] 毕林锐.核磁共振测井技术的最新若干进展[J].工程地球物理学报,2007,4(4):369-374.Bi L R.Latest advances in NMR logging technology[J].Chinese Journal of Engineering Geophysics,2007,4(4):369-374.

[10] 谭茂金,邹友龙,刘兵开,等.气水模型(T2,D)二维核磁共振测井数值模拟及参数影响分析[J].测井技术,2011,35(2):130-136.Tan M J,Zou Y L,Liu B K,et al.Inversions imulation of (T2,D) 2D NMR logging and analysis of observation parameters effects in gas-water model[J].Well Logging Technology,2011,35(2):130-136.

[11] 张世懋,葛祥,王辛,等.川西气田白云岩储层二维核磁共振测井气水识别方法[J].波谱学杂志,2020,37(3):360-369.Zhang S M,Ge X,Wang X,et al.A two-dimensional NMR logging method for gas-water identification in dolomite reservoir of the western Sichuan gas field[J].Chinese Journal of Magnetic Resonance,2020,37(3):360-369.

[12] 张世懋,张哨楠,葛祥,等.川西致密气藏二维核磁共振测井优化设计与应用[J].波谱学杂志,2018,35(2):234-242.Zhang S M,Zhang S N,Ge X,et al.Optimal design and application of two-dimensional NMR logging in Chuanxi tight gas reservoir[J].Chinese Journal of Magnetic Resonance,2018,35(2):234-242.

[13] 侯克均,吴见萌,葛祥,等.基于二维核磁共振弛豫谱的雷四段孔隙度计算方法[J].波谱学杂志,2020,37(2):162-171.Hou K J,Wu J M,Ge X,et al.Calculating porosity from two-dimensional NMR relaxation spectra of the leikoupo group’s 4th section[J].Chinese Journal of Magnetic Resonance,2020,37(2):162-171.

[14] 宁从前,周明顺,成捷,等.二维核磁共振测井在砂砾岩储层流体识别中的应用[J].岩性油气藏,2021,33(1):267-274.Ning C Q,Zhou M S,Cheng J,et al.Application of 2D NMR logging in fluid identification of glutenite reservoir[J].Lithologic Reservoirs,2021,33(1):267-274.

[15] 谭茂金,邹友龙.(T2,D)二维核磁共振测井混合反演方法与参数影响分析[J].地球物理学报,2012,55(2):683-692.Tan M J,Zou Y L.A hybrid inversion method of(T2,D) 2D NMR logging and observation parameters effects[J].Chinese Journal of Geophysics,2012,55(2):683-692.

[16] 孙中良,李志明,申宝剑,等.核磁共振技术在页岩油气储层评价中的应用[J].石油实验地质,2022,44(5):930-940.Sun Z L,Li Z M,Shen B J,et al.NMR technology in reservoir evaluation for shale oil and gas[J].Petroleum Geology & Experiment,2022,44(5):930-940.

[17] 高明哲,邹长春,彭诚,等.页岩储层岩心核磁共振实验参数选取方法研究[J].工程地球物理学报,2016,13(3):263-270.Gao M Z,Zou C C,Peng C,et al.Study on selection method of core nuclear magnetic resonance experiment parameters for shale reservoir[J].Chinese Journal of Engineering Geophysics,2016,13(3):263-270.

[18] 李嫣然,胡志明,刘先贵,等.泸州地区龙马溪组深层页岩孔隙结构特征[J].断块油气田,2022,29(5):584-590.Li Y R,Hu Z M,Liu X G,et al.The pore structure characteristics of deep shale in Longmaxi Formation of Luzhou area[J].Fault-Block Oil & Gas Field,2022,29(5):584-590.

[19] 杨文新,李继庆,赵江艳,等.四川盆地涪陵地区龙马溪组页岩微观孔隙结构定性定量研究[J].石油实验地质,2018,40(1):97-102.Yang W X,Li J Q,Zhao J Y,et al.Qualitative and quantitative study of micro-pore structures of Longmaxi Formation shale in Fuling area,Sichuan Basin[J].Petroleum Geology & Experiment,2018,40(1):97-102.

[20] 张烈辉,郭晶晶,唐洪明,等.四川盆地南部下志留统龙马溪组页岩孔隙结构特征[J].天然气工业,2015,35(3):22-29.Zhang L H,Guo J J,Tang H M,et al.Pore structure characteristics of Longmaxi shale in the southern Sichuan Basin[J].Natural Gas Industry,2015,35(3):22-29.

[21] 龚小平,唐洪明,赵峰,等.四川盆地龙马溪组页岩储层孔隙结构的定量表征[J].岩性油气藏,2016,28(3):48-57.Gong X P,Tang H M,Zhao F,et al.Quantitative characterization of pore structure in shale reservoir of Longmaxi Formation in Sichuan Basin[J].Lithologic Reservoirs,2016,28(3):48-57.

[22] Chi L,Heidari Z.Quantifying the impact of natural fractures and pore structure on NMR measurements in multiple-porosity systems[C]//International Petroleum Technology Conference.Doha,Qatar.IPTC,2014:IPTC-17688-MS.

[23] 王子萌,蒋裕强,付永红,等.基于核磁共振表征渝西地区五峰组-龙一1亚段页岩储层孔隙结构及非均质性[J].地球科学,2022,47(2):490-504.Wang Z M,Jiang Y Q,Fu Y H,et al.Characterization of pore structure and heterogeneity of shale reservoir from Wufeng Formation-sublayers Long-11 in western Chongqing based on nuclear magnetic resonance[J].Earth Science,2022,47(2):490-504.

[24] Ozeni A E,Sigal R F.T1/T2 NMR surface relaxation ratio for hydrocarbon sand brines in contact with mature organic-shale reservoir rocks[J].Petrophysics:The SPWLA Journal of Formation Evaluation and Reservoir Description,2013,54(1):11-19.

[25] Washburn K E ,Birdwell J E ,Seymour J D ,et al.Low-field nuclear magnetic resonance characterization of organic contentinshales[C]// lnternational Symposium of the Society of Core Analysts.NapaValley,Canada:Society of core Analysts,2013,

[26] Fleury M,Romero-Sarmiento M.Characterization of shalesusing T2-T1 nmr maps[J].Journal of Petroleum Science and Engineering,2016,137:55-62.

[27] 舒志国,关红梅,喻璐,等.四川盆地焦石坝地区页岩气储层孔隙参数测井评价方法[J].石油实验地质,2018,40(1):38-43.Shu Z G,Guan H M,Yu L,et al.Well logging evaluation of pore parameters for shale gas reservoirs in Jiaoshiba area,Sichuan Basin[J].Petroleum Geology & Experiment,2018,40(1):38-43.

[28] 芮昀,王长江,张凤生,等.昭通国家级页岩气示范区页岩气储层微观孔喉表征[J].天然气工业,2021,41(S1):78-85.Rui Y,Wang C J,Zhang F S,et al.Microscopic pore throat characterization of shale gas reservoir in Zhaotong national shale gas demonstration zone[J].Natural Gas Industry,2021,41(S1):78-85.

[29] 郭旭升,胡东风,李宇平,等.涪陵页岩气田富集高产主控地质因素[J].石油勘探与开发,2017,44(4):481-491.Guo X S,Hu D F,Li Y P,et al.Geological factors controlling shale gas enrichment and high production in Fuling shale gas field[J].Petroleum Exploration and Development,2017,44(4):481-491.

[30] 郭旭升,李宇平,腾格尔,等.四川盆地五峰组—龙马溪组深水陆棚相页岩生储机理探讨[J].石油勘探与开发,2020,47(1):193-201.Guo X S,Li Y P,Tenger,et al.Hydrocarbon generation and storage mechanisms of deep-water shelf shales of Ordovician Wufeng Formation-Silurian Longmaxi Formation in Sichuan Basin,China[J].Petroleum Exploration and Development,2020,47(1):193-201.

[31] 张福,黄艺,戴岑璞,等.黔北地区五峰组—龙马溪组页岩储层特征分析[J].天然气勘探与开发,2020,43(3):94-101.Zhang F,Huang Y,Dai C P,et al.Characteristics on shale reservoirs of Wufeng-Longmaxi Formations,northern Guizhou Province[J].Natural Gas Exploration and Development,2020,43(3):94-101.

[32] 郭世钊,郭建华,刘辰生,等.黔北地区志留系下统龙马溪组页岩气成藏潜力[J].中南大学学报(自然科学版),2016,47(6):1 973-1 980.Guo S Z,Guo J H,Liu C S,et al.Shale gas accumulation potential of Lower Silurian Longmaxi Formation in northern Guizhou[J].Journal of Central South University (Science and Technology),2016,47(6):1 973-1 980.

[33] 贺永忠,向坤鹏,安亚运,等.黔北正安地区五峰组—龙马溪组页岩气地质特征及有利区预测[J].中国地质调查,2020,7(3):21-29.He Y Z,Xiang K P,An Y Y,et al.Geological characteristics and favorable areas prediction of shale gas in Wufeng-Longmaxi Formation in Zheng’an area of Northern Guizhou[J].Geological Survey of China,2020,7(3):21-29.

[34] 谷阳,徐晟,徐佳佳,等.黔北地区下志留统龙马溪组页岩储层特征[J].断块油气田,2021,28(1):33-39.Gu Y,Xu S,Xu J J,et al.Shale reservoir characteristics of the lower Silurian Longmaxi Formation in northern Guizhou[J].Fault-Block Oil & Gas Field,2021,28(1):33-39.

[35] 刘治成,李红佼,张喜,等.川南—黔北地区下志留统龙马溪组沉积相展布及演化[J].沉积与特提斯地质,2021,41(3):436-445.Liu Z C,Li H J,Zhang X,et al.Distribution and evolution of sedimentary facies of the Lower Silurian Longmaxi Formation in southern Sichuan and northern Guizhou area[J].Sedimentary Geology and Tethyan Geology,2021,41(3):436-445.

[36] 翟刚毅,包书景,庞飞,等.贵州遵义地区安场向斜“四层楼”页岩油气成藏模式研究[J].中国地质,2017,44(1):1-12.Zhai G Y,Bao S J,Pang F,et al.Peservoir-forming pattern of “four-storey” hydrocarbon accumulation in Anchang syncline of northern Guizhou Province[J].Geology in China,2017,44(1):1-12.

[37] 雷子慧,赵安坤,余谦,等.贵州北部安场向斜下志留统龙马溪组页岩气保存条件[J].地质科技情报,2016,35(4):121-127.Lei Z H,Zhao A K,Yu Q,et al.Preservation of shale gas in lower Silurian Longmaxi Formation in Anchang syncline unit in northern Guizhou,South China[J].Geological Science and Technology Information,2016,35(4):121-127.

[38] 魏祥峰,刘珠江,王强,等.川东南丁山与焦石坝地区五峰组—龙马溪组页岩气富集条件差异分析与思考[J].天然气地球科学,2020,31(8):1 041-1 051.Wei X F,Liu Z J,Wang Q,et al.Analysis and thinking of the difference of Wufeng-Longmaxi shale gas enrichment conditions between Dingshan and Jiaoshiba areas in southeastern Sichuan Basin[J].Natural Gas Geoscience,2020,31(8):1 041-1 051.

[39] 郭彤楼,蒋恕,张培先,等.四川盆地外围常压页岩气勘探开发进展与攻关方向[J].石油实验地质,2020,42(5):837-845.Guo T L,Jiang S,Zhang P X,et al.Progress and direction of exploration and development of normally-pressured shale gas from the periphery of Sichuan Basin[J].Petroleum Geology & Experiment,2020,42(5):837-845.

[40] 周尚文,刘洪林,闫刚,等.中国南方海相页岩储层可动流体及T2截止值核磁共振研究[J].石油与天然气地质,2016,37(4):612-616.Zhou S W,Liu H L,Yan G,et al.NMR research of movable fluid and T2 cutoff of marine shale in South China[J].Oil & Gas Geology,2016,37(4):612-616.

[41] 李彤,郭和坤,李海波,等.致密砂岩可动流体及核磁共振T2截止值的实验研究[J].科学技术与工程,2013,13(3):701-704.Li T,Guo H K,Li H B,et al.Experimental research on movable fluid and NMR T2,cutoff in tight sandstone[J].Science Technology and Engineering,2013,13(3):701-704.

[42] 汪中浩,章成广,肖承文,等.低渗透储层T2截止值实验研究及其测井应用[J].石油物探,2004,43(5):508-510+414.Wang Z H,Zhang C G,Xiao C W,et al.T2 cutoff value in low-permeability reservoirs and its application[J].Geophysical Prospecting for Petrole,2004,43(5):508-510+414.

[43] 姜鹏,郭和坤,李海波,等.低渗透率砂岩可动流体T2截止值实验研究[J].测井技术,2010,34(4):327-330.Jiang P,Guo H K,Li H B,et al.Experimental study on T2 cutoff in low permeability sandstones[J].Well Logging Technology,2010,34(4):327-330.

[44] 闫子旺,张红玲,周晓峰,等.鄂尔多斯盆地西南部长8超低渗透砂岩核磁共振T2截止值研究[J].石油地质与工程,2015,29(5):128-131.Yan Z W,Zhang H L,Zhou X F,et al.Study on T2 cutoff value of nuclear magnetic resonance of Chang 8 ultra-low permeability sandstone in southwest Ordos Basin[J].Petroleum Geology and Engineering,2015,29(5):128-131.

[45] 朱明,贾春明,穆玉庆,等.基于正态分布拟合的致密砂砾岩储层核磁共振测井可变T2截止值计算方法[J].石油地球物理勘探,2021,56(3):612-621+416.Zhu M,Jia C M,Mu Y Q,et al.A method of predicting T2 cutoffs from NMR logging data of tight glutenite reservoirs based on normal distribution simulation[J].Oil Geophysical Prospecting,2021,56(3):612-621+416.

[46] 张海杰,蒋裕强,周克明,等.页岩气储层孔隙连通性及其对页岩气开发的启示——以四川盆地南部下志留统龙马溪组为例[J].天然气工业,2019,39(12):22-31.Zhang H J,Jiang Y Q,Zhou K M,et al.Connectivity of pores in shale reservoirs and its implications for the development of shale gas:A case study of the Lower Silurian Longmaxi Formation in the southern Sichuan Basin[J].Natural Gas Industry,2019,39(12):22-31.

[47] Keating K,Knight R.A laboratory study of the effect of Fe(II)-bearing minerals on nuclear magnetic resonance (NMR) relaxation measurements[J].Geophysics,2010,75(3):F71-F82.

[48] Saidian M,Prasad M.Effect of mineralogy on nuclear magnetic resonance surface relaxivity:A case study of middle bakken and three Forks formations[C]//SPE Annual Technical Conference and Exhibition.Houston,Texas,USA.Society of Petroleum Engineers,2015.DOI:10.2118/175052-ms.

[49] 吴丰,司马立强,令狐松,等.昆北地区储层核磁共振孔隙度偏低分析及校正[J].特种油气藏,2014,21(2):75-79+154.Wu F,Sima L Q,Linghu S,et al.Analysis and correction of low reservoir porosity derived from NMR log in the Kunbei area[J].Special Oil & Gas Reservoirs,2014,21(2):75-79+154.

[50] 李海燕,屈翠侠,刘斌,等.优势渗流层段测井评价及应用[J].工程地球物理学报,2024,21(5):855-865.Li H Y,Qu C X,Liu B,et al.Logging identification and evaluation of dominant seepage intervals[J].Chinese Journal of Engineering Geophysics,2024,21(5):855-865.

基本信息:

中图分类号:P631.81;P618.13

引用信息:

[1]吴晓光,李德才,樊靖宇,等.二维核磁共振测井在页岩储层评价中的应用[J].工程地球物理学报,2025,22(06):664-674.

基金信息:

中石化石油工程公司项目(编号:SG23-54K)

检 索 高级检索

引用

GB/T 7714-2015 格式引文
MLA格式引文
APA格式引文